FOB Price
Get Latest Price85 ~ 100 USD / Kilogram ( Negotiable )
|1 Ton Minimum Order
Country:
USA
Model No:
SILICA Quartz Lumps
FOB Price:
85 ~ 100 USD / Kilogram ( Negotiable )Get Latest Price
Place of Origin:
AFRICA - SAUDI ARABIA
Price for Minimum Order:
85 per Kilogram
Minimum Order Quantity:
1 Ton
Packaging Detail:
JUTE BAGS-75 POUND
Delivery Time:
IMMEDIATE
Supplying Ability:
100 Ton per Month
Payment Type:
Other, PayPal, Money Gram, Western Union, D/P, L/C, T/T
Product Group :
-
Contact Person L L
Las Vegas, Nevada
X-ray fluorescence spectrometry analysis
The analyses were performed using the XRF Wavelength Dispersive
Spectrometer (WDS-XRF) Philips PW***0, supplied to the Department
of Earth Sciences. The analytical methodology used is that
developed by Franzini et al. (***5). The accuracy of the analyses
is less than 2%. The total iron was determined as Fe2O3. The Loss
on Ignition (LOI) was determined by calcination at ***0°C for at
least 1 hour of approximately 1 g of sample.
The analytical results obtained from the X-ray fluorescence
spectrometry analysis were calibrated using calibration curves
obtained by measuring a series of about *0 international standard
certificates and some internal standards for high content of
SiO2.
Quartz 1 Quartz 2
Major (% weight)
SiO2
*9.*2 *9.*1
TiO2
<0.*1 <0.*1
Al2O3 0.*7
0.*8
Fe2O3tot
0.*3
0.*2
MnO <0.*1
<0.*1
MgO
0.*3 <0.*1
CaO
0.*3 0.*4
Na2O
0.*1 0.*2
K2O
<0.*1 <0.*1
P2O5 <0.*1
<0.*1
L.O.I.
0.*2 0.*3
Trace (ppm)
Ni
4 3
Co
<3 <3
Cr
6 5
V
<3 <3
Ce
<3
<3
Nd
<3 <3
Ba
<*0 <*0
La
<3 <3
Nb
<2
<2
Zr
<5 <5
Y
<4 <4
Sr
<6
<6
Rb
4
4
Pb
<2 <2
As
<3 <3
Zn
<2 <2
Cu
<*5
<*5
S
<*0 <*0
Cl
<*0
<*0
ICP - MS Qualitative Analysis
The determination was carried out using the Thermo Fisher
Scientific inductively coupled plasma Mass Spectrometer, X Series
II, supplied to the Centro Interdipartimentale Grandi Strumenti
[Interdepartmental Large Instruments Center]. The two samples were
prepared in solution in Pt crucibles by means of alkaline fusion
with LiBO2, in order to completely disperse the sample in a glass
matrix; subsequently the fusion obtained was solubilized in HNO3
and the solution analyzed by ICP-MS instrumentation.
The spectra reported in Figures 1 and 2 show the presence of many
trace or ultra-trace elements, as expected for samples of natural
origin.
Although using pure reagents (LiBO2 flux and solubilizing HNO3) for
the analysis, the level of impurities present in the reagents
caused however, given the high sensitivity of the instrumentation,
a significant disturbance on the instrument output, as evidenced by
the "blank" spectrum (blank = solution prepared using only the same
amount of flux and solubilizer used for the dissolution of the
samples) in Figures 1 and 2.
Therefore the identification of the ultra-trace components present,
certainly attributable to the matrix of the two samples, is not
certain with this type of qualitative analysis. In any case, other
than the elements for which the quantitative determination was done
with X-ray Fluorescence Spectrometry, other elements should not be
present in significant concentrations. In the event a quantitative
evaluation of ultra-trace elements becomes necessary the request
should be aimed at very specific groups of elements, and use
therefore of targeted solubilization procedures with high purity
reagents and standard solutions prepared ad hoc.
Bibliographical references
Franzini M., Leoni L. & Saitta M., (***5): Revision of a
fluorescence analytical methodology, based on the complete
correction of matrix effects. Rend. Soc. Ital. Mineral. Petrol.
[Reports of the Italian Mineralogical and Petrological Society],
*1, p. ******8.
Country: | USA |
Model No: | SILICA Quartz Lumps |
FOB Price: | 85 ~ 100 / Kilogram ( Negotiable ) Get Latest Price |
Place of Origin: | AFRICA - SAUDI ARABIA |
Price for Minimum Order: | 85 per Kilogram |
Minimum Order Quantity: | 1 Ton |
Packaging Detail: | JUTE BAGS-75 POUND |
Delivery Time: | IMMEDIATE |
Supplying Ability: | 100 Ton per Month |
Payment Type: | Other, PayPal, Money Gram, Western Union, D/P, L/C, T/T |
Product Group : | - |